AIR POLLUTION
CONTROL
INTRODUCTION
Air pollution is one of the most
serious environmental problems this planet is facing nowadays. Human
activities have drastically changed the air we are breathing by introducing materials
into the atmosphere in a great quantity every second, and subsequently changed
the entire environment (e.g. weather, ecosystem). As the residents in the
planet, human beings are unavoidably affected by this change (e.g. health
problems, reduced visibility, property damage). To improve the
environment and the quality of our life, it is important to develop
technologies to control the air pollution we produce.
In our research on
air pollution, we focus on the (1) understanding the mechanisms of pollutant
formation, and (2) development of new technology to control air pollution,
especially using aerosol science and particle technology. Following are
some examples.
METAL BEHAVIOR IN COMBUSTION SYSTEMS
Heavy metals such as lead, arsenic or
mercury are present in the waste we incinerate or coal we burn to generate
energy. Although they are in trace amount, they pose significant adverse
health problems because of their high toxicity. Unlike organic compounds,
these metals are destroyed in combustion systems and typically they will form
fine particles due to their high boiling points. However, the formation
depends on the operating conditions of the combustor (e.g. temperature) and the
materials in the combustor (e.g. chlorine content). To better control
them in combustion system, the first step is to understand their behavior in
combustion systems. Thermodynamic calculations and experiments are
conducted to evaluate the behavior of these metals in combustion systems. They are also used to evaluate the impact of
the components in flue gas such as HCl and SO2.
Related Publication:
1.
Wu, C. Y. and Biswas, P., "An Equilibrium
Analysis to Determine the Speciation of Metals in an Incinerator", Combustion
and Flame, 93, 31-40, 1993.
DEVELOPMENT OF INNOVATIVE SORBENT
TECHNOLOGY TO CONTROL HEAVY METALS
Sorbent materials, such as Al2O3,
SiO2 or TiO2, have been found to be effective to remove
heavy metals. Bulk materials such as bauxite or kaolinite
have been used. However, their effective area is on the surface and hence
a high quantity is required to control the heavy metal emission. Using an
aerosol technology, agglomerated sorbent materials with a much larger surface
area can be generated to in-situ capture heavy metals in combustion environment. Currently,
the foci of the group are: (1) CCA-treated wood (Cr, Cu and As)
and (2) As, Mo and V from coal combustion.

Related Publication:
2.
Owens,
T., Wu, C. Y. and Biswas, P., "An Equilibrium Analysis for
Reactions of Metal Compounds with Sorbents", Chemical Engineering
Communications, 133, 31-52, 1995.
3.
Biswas,
P. and Wu, C. Y., "Control of Toxic Metal Emissions from Combustors
using Sorbents: A Review", J. Air & Waste Management Association,
48, 113-127, 1998.
4.
Wu, C. Y. and Barton, T., "A Thermodynamic Equilibrium Analysis to
Determine the Potential Sorbent Materials for the Control of Arsenic Emissions
from Combustion Sources", Environmental
Engineering Science, 18(3),
179-192, 2001.
5.
Lee, S.
R. and Wu, C. Y., "Study of Vanadium Emission
Control in Combustion Systems by Thermodynamic Equilibrium Analyses", Advanced
in Environmental Research, 7(1), 1-10, 2002.
6.
Cho,
K. and Wu, C. Y., "Control of Molybdenum
Emission by Sorbents: An Equilibrium Analysis", submitted to J. Env.
7.
Iida,
K., Pierman, J., Tolaymat, T. Townsend, T. and Wu, C, Y., "Control of Heavy Metal Emissions and Leaching from
Incineration of CCA-Treated Woods Using Mineral Sorbents", submitted to J.
Env.
DEVELOPMENT OF NOVEL
CATALYST/PHOTOCATALYST TO CONTROL MERCURY EMISSION
Mercury is a unique metal in
combustion systems. While most other
metals are emitted as particulate matters, mercury is mainly emitted as
elemental mercury vapor, especially from coal fired power plants. Therefore, particle control devices are not
capable of capturing it. Meanwhile, it
is insoluble, making scrubber useless in removing it from flue gas. Currently, EPA has specified Activated Carbon
to be the Maximum Available Control Technology.
However, it’s not an ideal material (e.g. it requires 3 kg of the
best carbon to remove 1 g of Hg). Hence,
advanced technologies are being developed for effective capture of mercury in
combustion systems.
The major process involves
oxidation using strong oxidants such as hydroxyl radicals. Under UV light, semiconductor materials such
as TiO2 or ZnO can generate reactive hydroxyl radicals on their
surface that can be used to oxidize mercury (forming mercury oxide). Mercury oxide is attached to the surface of
the photocatalyst and is also more soluble (hence more desired). One application of the material is to in-situ
generate nano-photocatalyst in agglomerated form, thus the surface area is
high. The other way that is being
developed is to use nano-structured silica network doped with TiO2
that will have both functions of adsorption and photocatalysis. The third process being developed is to add a
third function which is to facilitate recycle and reuse of the material. Ultimately, a “smart” material
will be developed to detect, remove and signal the completion of its mission
(i.e. the system is clean of Hg or other pollutant).
Another materials being
investigated include nanosized Fe2O3 and CuO. They are activated by thermal energy instead
of photons. Therefore it is important to
identify the optimal temperature for the best performance. Additionally, these metal oxides can also be
engineered to improve their properties.

The mechanisms of the photocatalytic process in the system.
Related Publication:
8.
Wu, C. Y., Lee, T. G., Arar, E., Tyree, G. and
Biswas, P., "Capture of Mercury in Combustion Environments by In-Situ
Generated Titania Particles with UV Radiation", J. Environmental
Engineering Science, 15(2), 137-148, 1998.
9. Pitoniak, E., Wu, C. Y., Londeree, D., Mazyck, D., Bonzongo, J.-D., Powers, K. and Sigmund, W., “Nanostructured Silica-Gel Doped with TiO2 for Hg Vapor Control”, submitted to Journal of Nanoparticle Research, December 2002.
DEVELOPMENT OF HIGH SURFACE AREA
CATALYST FOR
Nanosized catalysts are
important in the control of automobile exhaust due to their high surface area
and reactivity. However, the application
requires their deposition on durable substrates. Currently the group is working on the development
of ceramic fiber coated with high surface area by coating binary nanosized
catalysts on the surface. The
experimental results show that a higher surface area fiber can be fabricated
with good dispersion of nanoparticles.



Raw fiber before processing Fiber
coated with 2% (wt) nanosized particles
DEVELOPMENT OF INNOVATIVE MAGNETIC
PHOTOCATALYST COMPOSITE
Photocatalyst such as TiO2
is a very effective material to decompose organic pollutants. Its application is important especially when
limited supply of chemicals is allowed.
In collaboration with other UF researchers, we developing photocatalyst
coated on magnet for use in microgravity environment. The developed composite can be used in
magnetic fluidization that does not rely on fluid flow.